freeslate jr. process chemistry

freeslate jr.

End old routines

Walk up, set up your run and walk away. Freeslate jr. turns reaction screening and process optimization into totally routine activities. Build a system for reaction screening and plow through hundreds of modifications per week. Deck one out with real-time sampling to fine-tune your chemistry pathways. Freeslate jr. lets you dive deep so you know exactly what tweaks to make next. Get brochure.

Process optimization

Screen continuous variables

Screen discrete variables

Optimize and screen synthetic routes

Improve yields and impurity profiles

Optimize catalyst loading

Map process robustness

freeslate_jr2

 

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Dial in your process

Freeslate jr. lets you check out a ton of reaction screening variables like solvents, ligands, catalysts and reagents all at once. It’ll plow through hundreds of modifications per week. Outfit one with an Optimization Sampling Reactor (OSR) to grab samples from your reactions as they’re happening and know even more right now. Get workflow guide.

FreeslateJR_proc_chem_components

1. Solvent tray
2. Optimization Sampling Reactor
3. 3-Position vortexing station
4. Wash station
5. Heating/cooling/stirring bay
6. 3-Position plate rack
 

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Find the sweet spot

Going the one variable at a time route doesn’t cut it when you need to know how all your different reaction variables play together. Add an Optimization Sampling Reactor (OSR) to freeslate jr. and get real-time kinetics on all your reactions. OSR grabs time-point samples from up to 8 pressure and temp-controlled vessels at a time without interrupting a single reaction. Each vessel makes sure the heating, cooling and stirring for each of your reactions is just right.

Optimization Sampling Reactor

Optimization Sampling Reactor

Cover all the bases

Freeslate jr. screens all your substrates, catalysts, reactants, solvents and reaction conditions so you can tackle a huge range of organic transformations. Dead-on dosing of small amounts of solids, liquids, slurries and viscous reagents keeps use of precious and expensive materials at an all-time low when prepping your reaction solutions. Tight reaction control, stir plate temps, filtration and dilution means your samples are ready for structural analysis whenever you are.

Heated 4-tip liquid dispenser

Heated 4-tip
liquid dispenser

Heating/cooling/stirring station

Heating/cooling/stirring station

Take reactions higher

Ultra-high temp and pressure reactions are no problem with the Screening Pressure Reactor (SPR). Run up to 96 experiments in parallel automatically and kick things up to 400 °C and 200 bar (3000 psig). Tie an SPR in with freeslate jr. for reaction screening and see if maxing temps and pressures gets your chemistry where you want it to go.

Screening Pressure Reactor

Screening Pressure Reactor

Break bottlenecks

LEA doesn’t move the bottleneck, it totally unclogs it. You get intuitive experimental design that makes sense on the front end and full integration with analytical tools on the back end. LEA also links your conditions, steps and analytical data together, so your final report doesn’t just have numbers, it’s got all the information you need to make real decisions. Learn more.

Already have a freeslate system? Download the latest version of LEA software.

LEA_process_chem

Videos

freeslate jr. for powder dispense (CMP Powder)